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【英文标准名称】:StandardTestMethodforSimultaneousMeasurementofSulfurCompoundsandMinorHydrocarbonsinNaturalGasandGaseousFuelsbyGasChromatographyandAtomicEmissionDetection
【原文标准名称】:用气相色谱法和原子发射检测法同步测量天然气和气体燃料中硫化合物和微量碳氢化合物的标准试验方法
【标准号】:ASTMD6968-2003(2009)
【标准状态】:现行
【国别】:美国
【发布日期】:2003
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:D03.05
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:
【英文主题词】:atomicemissiondetection;extendedgasanalysis;gaschromatography;hydrocarbons;odorants;sulfurcompounds;totalsulfur;Atomicemissiondetection;Extendedgasanalysis;Gaschromatography(GC)--petroleumproducts;Gaseousfuels;Hydrocarbons;
【摘要】:Gaseousfuels,suchasnaturalgas,petroleumgasesandbio-gases,containvaryingamountsandtypesofsulfurcompounds.Theyaregenerallyodorous,corrosivetoequipment,andcaninhibitordestroycatalystsemployedingasprocessing.Theiraccuratemeasurementisessentialtogasprocessing,operationandutilization,andmaybeofregulatoryinterest.Smallamounts(typically,1to4ppmv)ofsulfurodorantsareaddedtonaturalgasandotherfuelgasesforsafetypurposes.Somesulfurodorantscanbereactive,andmaybeoxidized,formingmorestablesulfurcompoundshavinglowerodorthresholds.Thesegaseousfuelsareanalyzedforsulfurodorantstohelpinmonitoringandtoensureappropriateodorantlevelsforpublicsafety.Thismethodoffersatechniquetodetermineindividualsulfurspeciesingaseousfuelandthetotalsulfurcontentbycalculation.Gaschromatographyiscommonlyandextensivelyusedtodetermineallcomponentsingaseousfuelsincludingfixedgasandorganiccomponents(TestMethodsD1945andD1946).Majorcomponentsmeasuredareoftenusedforthedeterminationofgasproperty,suchasheatingvalueandrelativedensity.Highermolarmasshydrocarbonsareofinterestevenwhenpresentinsmallamountsbecausetheirlargerimpactonheatingvalue,hydrocarbondewpointandgasqualityrelatingtogasoperation,gasutilizationandenvironmentalimpacts.1.1Thistestmethodisforthedeterminationofvolatilesulfur-containingcompoundsandminorhydrocarbonsingaseousfuelsincludingcomponentswithhighermolarmassthanthatofpropaneinahighmethanegas,bygaschromatography(GC)andatomicemissiondetection(AED).HydrocarbonsincludeindividualaliphaticcomponentsfromC4toC6,aromaticcomponentsandgroupsofhydrocarbonsclassifiedaccordingtocarbonnumbersuptoC12atleast,suchasC6-C7,C7-C8,C8-C9andC9-C10,etc.Thedetectionrangeforsulfurandcarboncontainingcompoundsisapproximately20to100000picograms(pg).Thisisroughlyequivalentto0.04to200mg/m3sulfurorcarbonbasedupontheanalysisofa0.25mLsample.1.2ThistestmethoddescribesaGC-AEDmethodemployingaspecificcapillaryGCcolumnasanillustrationfornaturalgasandothergaseousfuelcontaininglowpercentagesofethaneandpropane.AlternativeGCcolumnsandinstrumentparametersmaybeusedinthisanalysisoptimizedfordifferenttypesofgaseousfuel,providedthatappropriateseparationofthecompoundsofinterestcanbeachieved.1.3Thistestmethoddoesnotintendtoidentifyallindividualsulfurspecies.Unknownsulfurcompoundsaremeasuredasmono-sulfurcontainingcompounds.Totalsulfurcontentofasamplecanbefoundbysummingupsulfurcontentpresentinallsulfurspecies.1.4ThismethodisnotaDetailedHydrocarbonAnalysis(DHA)methodanddoesnotintendtoidentifyallindividualhydrocarbonspecies.Aliphatichydrocarboncomponentslighterthann-hexane,benzene,toluene,ethylbenzene,m,p-xylenesando-xylene(BTEX)aregenerallyseparatedandidentifiedindividually.Highermolarmasshydrocarbonsaredeterminedasgroupsbasedoncarbonnumber,excludingBTEX.Thetotalcarboncontentofpropaneandhighermolarmasscomponentsinasamplecanbefoundbysummingupcarboncontentpresentinallspeciescontainingcarbon.1.5ThevaluesstatedinSIunitsaretoberegardedasstandard.Nootherunitsofmeasurementareincludedinthisstandard.1.6Thisstandarddoesnotpurporttoaddressallof......
【中国标准分类号】:E24
【国际标准分类号】:75_160_30
【页数】:7P.;A4
【正文语种】:英语


【英文标准名称】:Guidetopreparationofmicrofilmandothermicroformsthatmayberequiredasevidence
【原文标准名称】:可用于作证的缩微胶卷与其他缩微胶片的制备指南
【标准号】:BS6498-1991
【标准状态】:作废
【国别】:英国
【发布日期】:1991-04-30
【实施或试行日期】:1991-04-30
【发布单位】:英国标准学会(BSI)
【起草单位】:
【标准类型】:()
【标准水平】:()
【中文主题词】:记录品(文献);验证;复制;法律文件;办公室管理;计算机输出缩微胶片;法规;记录品管理;缩微品;窗孔卡片;缩微胶卷;穿孔卡片;缩微照相
【英文主题词】:microphotography;microfilm;recordsmanagement;officemanagement;computeroutputonmicrofilm;legislation;microforms;records(documents);reprography;verification;legaldocuments;aperturecards
【摘要】:
【中国标准分类号】:A14
【国际标准分类号】:37_080
【页数】:16P;A4
【正文语种】:英语